Assign chemical shifts for a 14-residue peptide (TOCSY/NOESY data provided)

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I have a 14-residue peptide (sequence: CGSWTWENGKHTWK). I've collected NOESY/TOCSY data on a 400MHz machine. I require 3 things:

-Chemical shift assigment (for as many residues/atoms as possible)

-A figure showing the NOESY/TOCSY superposed spectra. Only the spectral region relevant to chemical shift assignment is needed. An example image for the same peptide in methanol is attached.

-A writeup on whatever methods you used to get the chemical shifts (1-2 paragraphs).

The figure & writeup must be publication quality.

Proof of NMR experience needed (institute affiliation, publications, etc) before accepting the project.

raw data here: [url removed, login to view]

Biologie Chemické inženýrství Vědecký výzkum

Identifikační číslo projektu: #16362724

O projektu

6 nabídek Projekt na dálku Aktivní před 5 lety

6 Freelnceři na tento projekt zveřejňují nabídky v průměru ₹29074

suyashdhoot

Hi I am Msc in medical biotechnology from IIT Bombay. I have 7 years of research and writing experience and have worked on PhD level thesis projects, published papers in peer reviewed journals and have also worked with Další

₹50000 INR za 10 dní
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5.1
ahaque126

hi there, please let me introduce myself as a seasoned organic chemist. I have more than 20 yrs of experience in the field. I am interested in your project. please let me know should you have any questions. with kind r Další

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MarcoPapaG

A proposal has not yet been provided

₹27777 INR za 10 dní
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youssefmahdhi91

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